Liquid NMR Facility Instruments

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NMR Facility Instrumentation Information

Webcal signup - reserve time for any instruments in facility

Instrument Information

Instrument-Specific Parameter Info

Siena - 400 MHz, VT (-80 - +130), multinuclear autotune, 12 position 7510 autosampler
Desk phone at Siena: Ext. 3014
Schedule: M-F 8 AM - 5 PM, 30 minutes; 5 PM - 8 AM unlimited
Weekend Schedule: 8 AM - 4 PM, 2 hours (sign up after 4 PM previous day); 4 PM - 8 AM, unlimited
FY2019 Internal Hourly Rate: $17.51

Hg2 - 300 MHz
No desk phone at Hg2; call Hg3 Ext. 8602
Schedule: 24 hours/day - 10 minutes except Fri 10 PM - Sat 8 AM & Sat 10 PM - Sun 8 AM, 1 hour
Weekend Schedule: n/a
FY2019 Internal Hourly Rate: $12.36

Hg3 - 300 MHz, 50 position SMS Autosampler
GLA: Nicholas Fastuca (nfastuca@caltech.edu
Desk phone at Hg3: Ext. 8602
Schedule: Monday to Friday 8 AM - 10 PM, 30 minutes; Monday to Thursday 10 PM - 8 AM, 4 hours; 
Friday 10  PM - 8 AM Monday, 8 hours
Signup required only for experiments more than 2 hours long.
FY2019 Internal Hourly Rate: $15.45

HgBI - 300 Mhz, VT (-80 - +130)
Location: 250 BI
Wall phone at HgBI: Ext. 2773
Schedule: M-F 8 AM - 11 PM, 30 minute; 11 PM - 8 AM, unlimited
Weekend Schedule: unlimited
FY2019 Internal Hourly Rate: $12.36

Daytona - 500 MHz, multinuclear, VT (-150 - +150)
Desk phone at Daytona: Ext. 8601
Schedule: 24 hours, sign up less than 72 hours in advance; longer times available upon request.
Weekend Schedule: same
FY2019 Internal Hourly Rate: $18.54

Indy - 500 MHz, 50 position SMS Autosampler
GLA: Austin Wright (awright@caltech.edu
Schedule: Every day 8 AM - 8 PM, 1 hour; every evening 8 PM - 11 PM, 2 hours; every night 11 PM - 8 AM, 9 hours (night queue)
Only sign up for night queue experiments on Indy's schedule, to verify the instrument is not overbooked. If there are samples in the night queue, the software will not accept new submissions between midnight and 8 am.
Weekend Schedule: same
FY2019 Internal Hourly Rate: $20.60

FID - 600 MHz, VT, inverse probes (i.e. higher proton sensitivity)
5 mm Penta PFG probe (H,C,P,N,D) is default, VT range -20 - +80
5 mm HCN Triax probe (backup only), VT range 0 - +50
3 mm inverse broadband PFG probe, VT range -20 - +80
Desk phone at FID: Ext. 8601
Schedule: 48 hours, sign up less than 72 hours in advance; longer times available upon request.
Weekend Schedule: same
FY2019 Internal Hourly Rate: $22.66

Florence - 400 MHz, 60 position SampleXpress sample changer, cryoprobe (i.e. higher sensitivity)
5 mm Prodigy cryoprobe (H/multinuclear from 31P to 15N) is default, VT range 0 - +80
5 mm SMART probe(H, F/multinuclear from 31P to 109Ag), VT range -150 - +150
GLA: David Schuman (dschuman@caltech.edu) Ext. 4047
Schedule: Day queue, 9 am - 9 pm daily, 46 minute maximum per experiment, 2.5 hours maximum per person. Night queue, 9 pm - 9 am, no limits.
You only need to sign up for the night queue, to verify the instrument is not overbooked. The samples will be run in the order they are submitted to the queue, not necessarily the order shown on the webcal schedule. If you are worried about the stability of a sample, you do not have to put it in the sample changer at the time of submission; you can wait until just before the time the sample will run.
FY2019 Internal Hourly Rate: $24.72

 

 

 FY2019 NMR Facility Rates

2019 NMR Facility Rates